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98, 228 (1976); Krusic, P. , Bingham, R. : J. Am. Chem. Soc. : J. Am. Chem. Soc. 99, 8348 (1977); McBride, J. : J. Am. Chem. Soc. 99, 6760 (1977); Claxton, T. , Symons, M. C. : Molecular Phys. 32, 1321 (1976); Dyke, J. et aL: Phys. Sci. A. 89, 107103 (1978); Griller, D. et aL: J. Am. Chem. Soe. 100, 6750, (1978). , Beckhaus, H. , Angew. Chem. 90, 635 (1978); Angew. Chem. Int. Ed. EngL 1 7, 594 (1978). In any case, all results point to much weaker force constants of out of plane deformations for free radicals than for earbenium ions.
07, Ref. 15. * 8 Me 93 K. A. 10. Ref. 09, Ref. 35. Ref. 11, 13)* l! 15)Sh, r _ 31 o 2 h, r_10 10 rain, Ref. 13)* t2 Me M~ eMe Me 15 94 from 2,2',4,4',6,6'-hexamethylstilbene, 4 x 10-4M, MCH/IH, h i 280 c 21% at +10 ~ Xma x (e)I: 475 (3100) II: 320 (7100), 310 (7000) III: 245 (15 800). tr. 4 (280). 1 I, 14) Me from 3,5,3',5'-tetramethylstilbene in MCH/IH UV a at - 1 8 0 ~ c 20%. 245 r_120 6 m i n ; r _ 1 6 0 = 43 rain Ref. 55) measured at - 1 8 0 ~. Ring opening with ;~ 436 at - 1 8 0 ~ * Ref. 15) T h e 4 a,4 b - D i h y d r o p h e n a n t h r e n e s Table 1 (continued) (~~OMe I6 see 4 m e t h o x y - D H P .
In Methods in Free Radical Chemistry (E. S. Huyser) Vol. 3, New York: Dekker 1972; Deno, N. , Pohl, D. : J. Org. Chem. 40, 380 (1975); J. Am. Chem. Soc. 96, 6680 (1974); b. : Synthesis 1973, 1; c. : J. Chem. Soe. B, 1968, 324; d. : Topics Curt. Chem. 62, 1 (1976); e. Johnson, R. , Green, F. : J. Org. Chem. 40, 2192 (1975) 71. , Wyckoff, J. : J. Am. Chem. Soc. 93, 2065 (1971) 72. Breslow, R. : J. Am. Chem. Soc. 94, 3277 (1972) 73. : Chem. Soc. Rev. 1, 553 (1972); Breslow, R. : J. Am. Chem. Soc.